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Beilstein J. Org. Chem. 2009, 5, No. 57, doi:10.3762/bjoc.5.57
Graphical Abstract
Scheme 1: Synthesis of tetraphenylenes 2.
Figure 1: DSC traces of compound 2h during (a) second cooling and (b) second heating (heating/cooling rate 5 ...
Figure 2: Texture of 2h under the POM at 25 °C upon cooling from the isotropic liquid (heating/cooling rate 5...
Figure 3: Molecular modelling of the saddle-shaped tetraphenylene (octakis)acyl core unit of 2 [35].
Figure 4: Clearing temperatures Tcl [°C] of tetraphenylenes 2e–l as a function of the chain lengths n.
Figure 5: The differences between the clearing temperatures Tcl [°C] of tetraphenylenes 2 and the melting poi...